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PHẢN ỨNG NGƯNG TỤ CLAISEN-SCHMIDT GIỮA ARYLMETHYL KETONES VÀ ARYLUNDER XÚC TÁC BỞI CU(OTF)2 TRONG ĐIỀU KIỆN KHÔNG DUNG MÔI: TỔNG HỢP CHALCONES
Tác giả: Đậu Xuân Đức, Nguyễn Thị Chung
631    37
Tạp chí khoa học và công nghệ
Quyển: 58; 6A     Trang: 1-9
Đường link/DOI: doi:10.15625/2525-2518/58/6A/15407
Minh chứng: 1202-clasen-schmidt.pdf
Năm xuất bản: 9/2020
Tóm tắt
An environmentally friendly and high yield method for the Claisen-Schmidt condensation has been investigated. A mixture of an arylmethyl ketone and an aldehyde was irradiated in a microwave reactor for 20 minute using Cu(OTf)2 as catalyst in solvent-free conditions. 12 chalcones were synthesized in moderate to excellent yields (74 - 91 %). This is the first time the Claisen-Schmidt condensation with Cu(OTf)2 under microwave irradiation is reported.
Từ khóa
bioactivity, benzaldehyde, acetophenone, irradiation, copper triflate.
Cùng tác giả
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